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008 091123s1996 si a sb 001 0 eng d
010 _z 97109494
040 _aWSPC
_beng
_cWSPC
020 _a9789812812124
_q(ebook)
020 _z9810225407
020 _z9789810225407
050 0 4 _aQD96.N8
_bK83 1996
082 0 4 _a543.66
_222
100 1 _aKudryavtsev, A. B.
245 1 0 _aPhysico-chemical applications of NMR :
_ba practical guide /
_cA.B. Kudryavtsev, W. Linert.
260 _aSingapore ;
_aRiver Edge, N.J. :
_bWorld Scientific Pub. Co.,
_cc1996.
300 _a1 online resource (xiv, 357 p.) :
_bill.
504 _aIncludes bibliographical references and index.
505 0 _ach. 1. NMR - Basic principles. 1.1. The phenomenon of nuclear magnetic resonance. 1.2. NMR spectra and their parameters. 1.3. Simplification of NMR spectra. 1.4. Analysis of NMR spectra. 1.5. Some hints on the mechanisms of relaxation and the nuclear Overhauser effect. 1.6. Physico-chemical aspects of the NMR. 1.7. Conclusion to chapter 1 -- ch. 2. Experimental techniques employed in NMR. 2.1. Introduction. 2.2. Principles of Fourier transform NMR spectroscopy. 2.3. Special features of the physico-chemical NMR experimental technique. 2.4. Routine of a typical PMR analysis of an organic compound -- ch. 3. The analysis of experimental data by regression techniques. 3.2. Introduction. 3.3. Definitions. 3.3. Least square fitting. 3.4. Non-linear least square methods -- ch. 4. Studies of equilibria in the liquid state by NMR spectroscopy. 4.2. Introduction. 4.2. Equilibria with slow exchange. 4.3. Equilibria with fast exchange -- ch. 5. Studies of paramagnetism in solutions by NMR. 5.1. Magnetochemistry. 5.2. Contact shifts -- ch. 6. Dynamic NMR and nuclear magnetic relaxation measurements. 6.1. Dynamic NMR. 6.2. Relaxation measurements.
520 _aThe book is intended to help under- and postgraduate students and young scientists in the correct application of NMR to the solution of physico-chemical problems concerning the study of equilibria in solution. The first part of the book (Chapters 1-3) is a trivium, but should enable a student to design and conduct simple physico-chemical NMR experiments. The following chapters give illustrative material on the physico-chemical applications of NMR of increasing complexity. These chapters include the problem of determination of equilibrium and rate constants in solution, the study of paramagnetism using NMR, the application of Dynamic NMR techniques and relaxation measurements. A multipurpose nonlinear regression program is supplied (on disc for PC) and is referred to throughout the book.
533 _aElectronic reproduction.
_bSingapore :
_cWorld Scientific Publishing Co.,
_d1996.
_nSystem requirements: Adobe Acrobat Reader.
_nMode of access: World Wide Web.
650 0 _aNuclear magnetic resonance spectroscopy.
655 0 _aElectronic books.
700 1 _aLinert, W.
710 2 _aWorld Scientific (Firm)
856 4 0 _uhttps://www.worldscientific.com/worldscibooks/10.1142/3004#t=toc
942 _cE-BOOK
999 _c49785
_d49785